Autotitrator ppt to pdf

Automatic potentiometric titrator at710m large color tftlcd with a touch panel 8. Karl fischer titration,principle,apparatus, titration types. In the volumetric titration method, iodine required for reaction with water is previously dissolved in water determination, and water content is. A titration curve is a curve in graph the xcoordinate of which represents the volume of titrant added since the beginning of the titration, and the ycoordinate of which represents the concentration of the analyte at the corresponding stage of the titration in an acidbase titration, the ycoordinate usually represents the ph of the solution. Make ppt and pptx slideshows easy to view by converting them to pdf. Autotitrator titration equivalence point detection. It is used to determine an unknown concentration of a known substance in a sample. Our patented electrode memory sotres all the calibration data and serial number with. Potentiometric titrations provide more reliable data than data from titrations that use chemical indicators and are particularly useful with colored or turbid solutions and.

Titrando is a highend potentiometric titrator that leaves nothing to be desired. Easyplus titration easy ph easy ox easy cl easy pro. Potentiometric titrations potentiometric titrations involves the measurement of the potential of a suitable indicator electrode with respect to a reference electrode as a function of titrant volume. This software allows to capture the data stored in the titrators at710b,at700,mka610, mkc610, at610 and at510 on a personal computer through cf memory card to manageanalyze titration results. Up to 4 titrators, mkv710b volumetric, mkc710b coulometric or mkh7102nd hybrid karl fischer moisture titrators or additional at710b potentiometric titrators, can be connected and simultaneous measurement is possible. Autotitrators are programmed to precisely add known amounts of a. Chapter 1 pharmaceutical quality system 31 january 20 chapter 2 personnel 16 february 2014. Highend titrator for potentiometric titration with two measuring interfaces for use with dosino dosing systems. The aut701 titrator can track users with access permissions, and track electrode calibration, serial number, date, time, operator, etc. A reagent, termed the titrant or titrator, is prepared as a standard solution of known concentration and volume. Procedure for calibration of autotitrator mettler toledo.

It was invented by a german chemist by name karl fischer in the year 1935. It provides an adaptable and highly accurate method to achieve high purity, essential to pharmaceuticals especially. And the las design is accomplished with minimum maintenance in view. After the completing of titration, the solution is discarded and the titration vessels are rinsed with water, washed and dried. Koehler k90500 k90590 tantbn titrator total acidbase.

Kf titrators t70 and t90, water determination has reached an unrivaled. Automatic titrators are best for accurate and repeatable results, as an electrochemical. Today, the titration is done with an automated karl fischer titrator. Titrando is the right titrator for any analytical requirement. The autotitrator that fails to meet the calibration limits is declared out of order and inform to service engineer. Automatic titration systems with cliplock exchangeable burette system and automatic burette recognition 6 titration. Product description for determination of total acid number tan, total base number tbn, saponification number, mercaptan sulfur, chloride content and karl fischer water content of petroleum products, lubricants, transformer insulating oils and crude oil. Honeywell confidential 2016 by honeywell international inc. A solution a so called titrant or standard solution is added to sample to be analyzed. Our titrator product offering includes electronic burettes, products for acidbase titrations, units with endpoint and equivalence point titration, meters for redox titrations, and products for karl fischer volumetric around 1% and coulometric at lower levels titrations. Titrators are used in nearly every imaginable industry doing chemical analyses, including petroleum and plastics, foods and beverages, paper, pharmaceuticals and biotechnology, cosmetics, electronics, automotive and aerospace, forensic labs, academia and more. Potentiometer construction, working and applications elprocus. A simple, rapid method for the quantitative estimation of secondary amines was developed based upon the reaction of this group of compounds with sodium. The advantages of potentiometric titration sciencing.

Sop for calibration of potentiometric titrator metrohm. Fundamentals of potentiometric titration is a threeday indepth course that leads the attendee through the basics, practical applications, operation and maintenance of potentiometric titration systems and electrodes. However, some of the disadvantages include the timeconsuming and laborintensive nature of measurements and the requirement of solutions of accurately known concentrations dimzon and knepper, 2015. Delivery tubes for digital titrator, 90 degree bend. Titrators we offer a variety of titrator products to meet your needs. Aut701 automatic titrators analyticon instruments corporation. Introductionvolumetric analysis simple and easy fast and can be done on site less expensive estimation of content or assay precise and accurate depends on method and specificity 3.

Potentiometer construction, working and applications the potentiometer is an electric instrument used to measure the emf electromotive force of a given cell, the internal resistance of a cell. Karl fischer titration is used for many substances as a reference method, and is a chemical analysis based on the oxidation of sulfur dioxide by iodine in a methanolic hydroxide solution. Use soda pdfs online converter tool and convert powerpoint to pdf for free. Extends the titrando, usb sample processors, dosing interface, titrosampler by two rs232 interfaces for connecting e. After necessary repairs the autotitrator is recalibrated before use. Single, multiple, and dynamically linked titration methods and routines. It was invented in 1935 by the german chemist karl fischer. Pharmaceutical analysis pharmaceutical analysis may be defined as the application of analytical procedures used to determine the purity, safety and quality of drugs and chemicals this course has access to the full range of titration method spectroscopic technique chromatographic method spectrophotometry etc. Save powerpoint presentations as pdf files office support. Saving your presentation as a pdf lets anyone view it, even if they dont have powerpoint.

The titrant reacts with a solution of analyte which may also be termed. Determination of salt food safety and inspection service. Water determination by karl fischer titration labicom. A typical set up for potentiometric titrations is given in figure 2. Kf titrator what is the meaning of karl fisher titration. The karl fischer titration anthony lucio the university of iowa shaw group meeting 3720 1. Standard operating procedure for calibration of autotitrator calibration of the burette, linearity and correlation coefficient. Standard operating procedure to check the performance of potentiometric titrator.

To calibrate the equipment for reliable and accurate results. Use of metrohm autotitrator in chm 286 and chm 315. Introductionvolumetric analysis simple and easy fast and can be done on site less expensive estimation of content or assay precise and accurate depends on method and specificity. The 916 titouch is the new compact titrator for potentiometric titration. Calculate the titratable acidity using the following formula. To do this, two electrodes are used, an indicator electrode the glass electrode and metal ion indicator electrode and a reference electrode. Download your new pdf and save it to your computer. Fischer titrators v20v30, c20c30 and excellence combined general and volumetric.

Autotitrators are programmed to precisely add known amounts of a chemical called the titrant to exactly quantify the amount of an unknown chemical the analyte in a sample. Hi 902 also features the addition of backtitration. Converting powerpoint files to pdfs has never been so easy. Up to 4 titrators, mkv710b volumetric, mkc710b coulometric or mkh7102nd hybrid karl fischer moisture titrators or additional at710b potentiometric titrators, can be connected and simultaneous measurement. As the silver nitrate solution is slowly added, a precipitate of silver. W446, rabale midc, rabale, navi mumbai 400701, maharashtra, india. Oct 26, 2016 for the love of physics walter lewin may 16, 2011 duration. No file size restrictions, no ad watermarks just a free online tool for creating pdfs from your ppt slides. Determination of chloride ion concentration by titration mohrs method 1 determination of chloride ion concentration by titration mohrs method introduction this method determines the chloride ion concentration of a solution by titration with silver nitrate. Titrator definition of titrator by the free dictionary.

When the conversion is done, your ppt, pptx, and pdf files will be automatically deleted. Its simplicity and accuracy ensure continued usefulness. Karl fischer titration is a classic titration method in analytical chemistry that uses coulometric or volumetric titration to determine trace amounts of water in a sample. Slideshare uses cookies to improve functionality and performance, and to provide you with relevant advertising. Titration is the fundamental chemical analysis procedure whereby the concentration of a chemical substance in solution is determined by. There are many types of titration methods which can be performed. And also it is used to compare the emfs of different cells. This procedure is applicable to the autotitrator as per operating procedure.

Ppt to pdf converter convert your powerpoint to pdf online free. Autotitrator titration equivalence point detection kinetics john c. Potentiometric titrations provide more reliable data than data from titrations that use chemical indicators and are particularly useful with colored or turbid solutions and for detecting the presence of unsuspected species. Water determination by karl fischer titration agnieszka kossakowska. If the switch off voltage is too low, too much iodine is added before the. Objective to lay down the procedure for calibration of autotitrator mettler toledo dl50. Full traceability and compliance glp, gmp, and fda 21 cfr part 11 extraordinary convenience. Det dynamic equivalence point titration, met monotone. With normal karl fischer titrators it must be determined experimentally. To check that the instrument performs satisfactorily and gives accurate and reproducible results. These techniques are the preset endpoint and equivalence point techniques, respectively.

To do this, two electrodes are used, an indicator electrode the glass electrode and metal ion. Titration also known as titrimetry and volumetric analysis is a common laboratory method of quantitative chemical analysis to determine the concentration of an identified analyte a substance to be analyzed. A titrator, or automatic titrator or autotitrator, is an analytical instrument used to automatically quantify the amount of a chosen substance in a sample. Automatic titrator automatic potentiometric titrator at710m large color tftlcd with a touch panel 8. Karl fischer titration guide for water moisture determination. The instrument supports the following titration modes. Determination of chloride ion concentration by titration. Automatic titrator, automatic potentiometric titrators.

Water determination by karl fischer titration agnieszka kossakowska praha, 03. History of karl fischer titration karl fischer march 24, 1901 april 16, 1958 was a german chemist published a method in 1935 to determine trace. Karl fischer titration is a classic titration method in chemical analysis that uses coulometric or volumetric titration to determine trace amounts of water in a sample. With the new generation of mettler toledo compact volumetric and coulometric karl fischer titrators v20v30, c20c30 and excellence combined general and volumetric. In 2014, hydranal technical service in seelze completed its combined accreditation according to isoiec 17025 and iso guide 34, the so. Potentiometric titration entails measuring the voltage change of a titration across a sample needing purification. Volumetry with volumetric titration the titrant is added to the sample by a burette from an external source. The autotitrator can find the ph endpoint in one of two ways. This sop is applicable for operation and calibration auto titrator metrohm. The basic principle of the titration is the following.

Potentiometric titration an overview sciencedirect topics. Potentiometric titrations involves the measurement of the potential of a suitable indicator electrode with respect to a reference electrode as a function of titrant volume. Jarubol chaichana bureau of drug and narcotic department of. Las analyzers may be thought of as an atline laboratory in a box complete with sampling, analysis, reportingalarming, cleanup, and even autocalibration for continuous, unattended operation. Methods include full auto for automatic end point detection and end level for preset endpoint level titrations. Jan 11, 2017 over view of pharmaceutical analysis 1. This presentation contains material of some parts in submarine. Karl fischer titration is the method of choice for water content determination. General european omcl network geon quality management document.

Automatic titrator aut701 display color graphic lcd with back light displayed item simultaneous indication of titration curve, titration volume, phmv, temperature and titration time changing over display of system asystem b display when dual system. Convert ppt to pdf in seconds using adobe acrobat online services. Young department of chemistry, saint marys university, halifax, nova scotia, canada b3h 3c3, john. The volume of titrant added to the sample is measured during the titration.

Karl fischer titration is a titration method which uses volumetric or coulometric titration to determine the trace quantity of water in the sample. Potentiometric titration is a technique similar to direct titration of a redox reaction. Select up to 5 products from below to compare or request more information. Tamperproof pdf reports can be created on the instrument and saved on a usb stick or directly transferred to your lims or intranet via ethernet connection. Potentiometric titration is considered to be the most consistent and robust technique among the nonnmr methods czechowskabiskup, 2012. Learn how to easily convert a microsoft powerpoint. Scope this sop shall be applicable for the autotitrator mettler toledo dl50. Compare and learn about automatic titrator autotitration autotitrator manufacturers on labcompare. Water determination with karl fischer titration principle.